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Influence of the nature of the electrolyte on the chiral separation of basic compounds in nonaqueous capillary electrophoresis using heptakis(2,3-di-O-methyl-6-O-sulfo)-beta-cyclodextrin.
Servais AC, Fillet M, Chiap P, Dewé W, Hubert P, Crommen J. Servais AC, et al. J Chromatogr A. 2005 Mar 11;1068(1):143-50. doi: 10.1016/j.chroma.2004.12.010. J Chromatogr A. 2005. PMID: 15844552 Free article.
The influence on the enantiomeric resolution of the nature of the cationic BGE component (sodium, ammonium or potassium) and that of the anionic component (chloride, formate, methanesulfonate or camphorsulfonate) as well as the concentration of heptakis(2,3-di-O-met …
The influence on the enantiomeric resolution of the nature of the cationic BGE component (sodium, ammonium or potassium) and that of …
Nonaqueous electrokinetic chromatography-electrospray ionization mass spectrometry using anionic cyclodextrins.
Mol R, Servais AC, Fillet M, Crommen J, de Jong GJ, Somsen GW. Mol R, et al. J Chromatogr A. 2007 Aug 3;1159(1-2):51-7. doi: 10.1016/j.chroma.2007.05.050. Epub 2007 May 18. J Chromatogr A. 2007. PMID: 17543975 Free article.
When a voltage is applied over the CE capillary, the overall mobility of the CDs is towards the inlet vial preventing CDs from entering the ion source. However, the sodium counter ions of the CDs still enter the ion source and appeared to cause ionization suppression. ...T …
When a voltage is applied over the CE capillary, the overall mobility of the CDs is towards the inlet vial preventing CDs from entering the …
Influence of the BGE composition on analyte response in CD-mediated NACE-MS.
Servais AC, Fillet M, Mol R, Rousseau A, Crommen J, Somsen GW, de Jong GJ. Servais AC, et al. Electrophoresis. 2010 Apr;31(7):1157-1161. doi: 10.1002/elps.200900649. Electrophoresis. 2010. PMID: 20209573
Addition of single-isomer sulfated beta-CD derivatives (available as sodium salt) to the BGE revealed that the anionic CD derivatives did not give rise to the same ionization suppression effect. This result can be attributed to differences in the dissociation state of thes …
Addition of single-isomer sulfated beta-CD derivatives (available as sodium salt) to the BGE revealed that the anionic CD derivatives …